Chemistry of hydrocarbon compounds – Unsaturated compound synthesis – From nonhydrocarbon feed
Patent
1980-07-07
1982-05-25
Davis, Curtis R.
Chemistry of hydrocarbon compounds
Unsaturated compound synthesis
From nonhydrocarbon feed
585639, C07C 120
Patent
active
043318240
ABSTRACT:
Highly purified isobutylene, up to 99.9% pure, is obtained by treating a reaction mixture such as that recovered from an isobutylene-containing hydrocarbon mixture also containing an aqueous solution of an aliphatic carboxylic acid having 1 to 6 carbon atoms that has been reacted in an acidic ion exchanger and from which the unreacted hydrocarbons have been removed. The operative ingredients of the treated mixture are tertiary butyl alcohol, secondary butyl alcohol and their esters of the carboxylic acid employed. When treated with an acidic ion exchanger the carboxylic acid is first formed which inhibits the secondary butyl alcohol and secondary butyl ester of the acid from decomposing and high purity isobutylene is recovered therefrom by conventional distillation.
REFERENCES:
patent: 3510538 (1970-05-01), Rosenthal
patent: 4011272 (1977-03-01), Matsuzawa et al.
patent: 4178317 (1979-12-01), Horn et al.
patent: 4232177 (1980-11-01), Smith
Ikeda Minoru
Inoue Kazutaka
Yoshioka Teruhiko
Davis Curtis R.
Mitsubishi Rayon Co. Ltd.
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