Process for post reactor purging of residual monomers from solid

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Treating polymer containing material or treating a solid...

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C08F 628

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active

054789222

ABSTRACT:
A process for removing unpolymerized monomers from a solid olefin polymer containing the monomers by countercurrently feeding an inert purge gas through a bed of polymer in a cylindrical purge vessel having tapered walls wherein the vessel has a height to bottom diameter ratio of 0.5:1 to 10:1 and the walls have a tapered angle based on a vertical axis of 0.5 to 15 degrees. An apparatus for removing unpolymerized monomers from a solid olefin polymer containing the monomers which comprises, a cylindrical purge vessel having tapered walls wherein the vessel has a height to bottom diameter ratio of 0.5:1 to 10:1 and the walls have a tapered angle based on a vertical axis of 0.5 to 15 degrees; a solids inlet disposed in an upper portion of the vessel; a solids discharge disposed in a lower portion of the vessel; gas entry means disposed within or below a bed of solids, and gas discharge means disposed in the upper portion of the vessel.

REFERENCES:
patent: 3450183 (1969-06-01), Hinton
patent: 3594356 (1971-07-01), Hinton
patent: 4197399 (1980-04-01), Noel et al.
patent: 4372758 (1983-02-01), Bobst et al.
patent: 5292863 (1994-03-01), Wang

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