Process for monitoring and controlling nitrating processes...

Radiant energy – Invisible radiant energy responsive electric signalling – Infrared responsive

Reexamination Certificate

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Reexamination Certificate

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10769997

ABSTRACT:
A process for monitoring and/or controlling a nitrating process, having the following steps:measuring inline infrared spectra of nitric acid content in a reaction mixture stream downstream of the nitration reaction, preferably near-infrared spectra,evaluating the measured spectra by means of a computer-assisted, matrix-specific calibration model for the purpose of determining the content of nitric acid,transmitting the results of spectrometric examination to a process control system,inputting the results of spectrometric examination for the purpose of specifying the content of nitric acid in the acid phase into a regulator (224) for control of the metering (207,217) of nitric acid into a nitrating reactor.

REFERENCES:
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patent: 5679873 (1997-10-01), Klingler et al.
patent: 6072576 (2000-06-01), McDonald et al.
patent: 6103934 (2000-08-01), Hallinan et al.
patent: 6561010 (2003-05-01), Wilson et al.
patent: 6810718 (2004-11-01), Wilson et al.
patent: 2004/0249512 (2004-12-01), Meeuwssen et al.
David Firth, Nitration Reactions in the manufacture of Pharamceutircal Intermediates, Jan. 2001, Innovations in Pharamceutical Technology, pp. 132-139.

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