Process for measurement of the degree of cure and percent resin

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2503411, G01N 2135

Patent

active

054573190

ABSTRACT:
The degree of cure and the amount of epoxy resin in a glass fiber reinforced epoxy resin prepreg is measured by exposing the prepreg to a series of light pulses created by optical filters transmitting light at predetermined bandwidths about selected wavelengths, preferably centered at wavenumbers of about 4529 cm.sup.-1 and 4055 cm.sup.-1 and measuring the amount of epoxy groups and methyl groups present relative to reference values from the electrical pulses produced by a phase sensitive photoelectric detector disposed to receive said light pulses after being exposed to said prepreg. When such measurements are made in a continuously moving sheet of prepreg, it is possible to control the variation of percent cure and resin content to no greater than .+-.3% cure and .+-.3% resin content over a distance of at least 400 yds (366 m).

REFERENCES:
patent: 3970393 (1976-07-01), Krygeris et al.
patent: 4582520 (1986-04-01), Sturm
patent: 4609628 (1986-09-01), Aschenbeck
patent: 4769544 (1988-09-01), Dahlquist
patent: 5142151 (1992-08-01), Varnell et al.

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