Process for manufacture of pentaerythritol diphosphites

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Processes of preparing a desired or intentional composition...

Reexamination Certificate

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C558S078000, C568S012000

Reexamination Certificate

active

07342060

ABSTRACT:
A method is disclosed for the production of pentaerythritol diphosphites of high spiro isomer content. The pentaerythritol diphosphites are produced via sequential transesterification of pentaerythritol with a monophosphite followed by a substituted phenol or other alcohol, wherein the transesterification reactions are carried out under controlled conditions of temperature and pressure. The unique reaction conditions result in intermediate and final pentaerythritol diphosphites of high spiro isomer content and high total yield of the diphosphites.

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patent: 5438086 (1995-08-01), Stevenson et al.
patent: 5674927 (1997-10-01), Mahood
patent: 6613823 (2003-09-01), Battiste et al.
patent: 6656887 (2003-12-01), Yagishita et al.
patent: 6657025 (2003-12-01), Blackmon et al.
patent: 6657032 (2003-12-01), Vanderbilt
patent: WO 03/102004 (2003-12-01), None

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