Process for manufacture of dense neodymium stabilized...

Compositions: ceramic – Ceramic compositions – Refractory

Reexamination Certificate

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C501S097400, C501S098200, C501S098300, C264S683000

Reexamination Certificate

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07109139

ABSTRACT:
The present invention provides a process for the manufacture of dense neodymium stabilized β-Si3N4-α-SiAlON composite, wherein a synergistic composition essentially consisting of Si3N4, Al2O3, AlN, SiO2and Nd2O3as starting materials is mixed in proportion to make a total of 100 mole in the mixed batch, passing the powder through 100 mesh, pressing the powder to form green compacts, sintering the green compacts at a temperature in the range of 1700° to 1900° C. in nitrogen atmosphere. The process of the present invention provides neodymium stabilized β-Si3N4-α-SiAlON composites by processing a composition from the system Si3N4—Al2O3.AlN—Nd2O3.9AlN—SiO2resulting into dense product of the order of >98% theoretical density with the advantages such as cost effectiveness, high hardness and high fracture toughness. The produced dense β-Si3N4-α-SiAlON will be useful for low temperature applications such as wear parts like bearing and roller materials and particularly for grinding and milling operations like grinding balls.

REFERENCES:
patent: 4421528 (1983-12-01), Buljan et al.
patent: 5032553 (1991-07-01), Tarry
patent: 5413972 (1995-05-01), Hwang et al.
patent: 5908798 (1999-06-01), Chen et al.
patent: 6824727 (2004-11-01), Roy et al.

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