Process for making vinyl pyrrolidone/vinyl acetate...

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Polymers from only ethylenic monomers or processes of...

Reexamination Certificate

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C526S071000, C526S212000, C526S264000, C526S330000

Reexamination Certificate

active

06939927

ABSTRACT:
Vinyl pyrrolidone/vinyl acetate copolymers having a very low residual vinyl pyrrolidone monomer level, i.e. <100 ppm, preferably only 50 ppm, are made within an advantageously short production cycle, by post-treating an aqueous solution of the copolymer at an elevated temperature of about 120–150° C., preferably about 130° C., under pressure, in the presence of a high temperature initiator, for a period of about 1–4 hours, preferably 2 hours.

REFERENCES:
patent: 5239053 (1993-08-01), Tseng et al.
patent: 5319041 (1994-06-01), Zhong et al.
patent: 5387641 (1995-02-01), Yeung et al.
patent: 5395904 (1995-03-01), Zhong et al.
patent: 5502136 (1996-03-01), Zhong et al.
patent: 5534564 (1996-07-01), Zhong et al.

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