Process for making solid formulations containing amine oxide sur

Compositions – Fluent dielectric – N-containing

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252546, 25217419, 564298, 562582, C11D 175, C11D 320, C07C 59245, C07C29100

Patent

active

053893069

ABSTRACT:
Disclosed is a process for making solid formulations containing amine oxide surfactants. Maleic acid, or a water soluble salt thereof, is admixed with an aqueous liquid amine oxide formulation, which formulation preferably contains from about 20% to about 40% by weight of an amine oxide surfactant. The molar ratio of maleic acid to amine oxide surfactant is at least about 1:1. Admixture pH is maintained at or below, or reduced to at least, about 1 unit below the pKa of the amine oxide to form a visible precipitate therein. The precipitate is separated from the mixture, preferably by mechanical means, and dried. The dried precipitate is a maleic acid-amine oxide salt which can be incorporated into cleaning products, especially solid or granular cleaning products, as a source of amine oxide surfactant.

REFERENCES:
patent: 3275673 (1966-09-01), Barlow
patent: 3983079 (1976-09-01), Spadini et al.
patent: 4320033 (1982-03-01), Yoshikawa
patent: 4338216 (1982-07-01), Earl et al.
patent: 5075501 (1991-12-01), Borland et al.
patent: 5130488 (1992-07-01), Smith et al.
English Abstract of Japan Patent Document JP 4904282, Apr. 18, 1974, Derwent Publications Ltd., Derwent data base accession No. 74942V/43.

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