Chemistry of inorganic compounds – Sulfur or compound thereof – Oxygen containing
Patent
1975-03-27
1976-11-30
Thomas, Earl C.
Chemistry of inorganic compounds
Sulfur or compound thereof
Oxygen containing
C01D 514
Patent
active
039950158
ABSTRACT:
Improvement in the process for making sodium metabisulfite by contacting a suspension of sodium carbonate in countercurrent stream with sulfur dioxide, which involves passing sulfur dioxide-containing gas sequentially through a first and a second reaction vessel, maintaining an acidic aqueous slurry of sodium metabisulfite in the first reaction vessel and a strongly alkaline aqueous slurry of sodium carbonate in the second reaction vessel, continuously feeding sodium carbonate to the second reaction vessel, passing strongly alkaline slurry from the second reaction vessel to the first reaction vessel and overflowing excess liquid from the first reaction vessel to the second reaction vessel, and recovering sodium metabisulfite crystals from the slurry in the first reaction vessel.
REFERENCES:
patent: 1638492 (1927-08-01), Laury
patent: 2245697 (1941-06-01), Melendy
patent: 3361524 (1968-01-01), Spormann et al.
patent: 3369866 (1968-02-01), Spormann et al.
patent: 3860695 (1975-01-01), Metzger et al.
Allied Chemical Corporation
Fuchs Gerhard H,.
Rooney Gerard P.
Thomas Earl C.
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