Process for making salt-free amphoterics with high mono amphopro

Cleaning compositions for solid surfaces – auxiliary compositions – Cleaning compositions or processes of preparing – Specific organic component

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510501, 554 63, 554 66, C11D 110

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active

060309385

ABSTRACT:
A novel, salt-free monoamphopropionate amphoteric surfactant is prepared in yields of from 75% to 80%, from a reaction comprising an imidazoline and a mixture of acrylic acid and sodium acrylate in an aqueous medium. The acrylic acid/sodium acrylate mixture is comprised of the two components in a range of molar ratios of from about 1:6 to about 1:3, respectively, and by replacing methyl acrylate, the reaction does away with the production of methanol which is an unwanted, hazardous and toxic byproduct. The imidazoline reacts in amounts in excess of 90% resulting in the highly pure yields and any left over unreacted acrylic acid can be easily removed by treating it with sodium bisulfate.

REFERENCES:
patent: 2374354 (1945-04-01), Kaplan
patent: 2524218 (1950-10-01), Bersworth
patent: 2530147 (1950-11-01), Bersworth
patent: 2532391 (1950-12-01), Bersworth
patent: 2568876 (1951-09-01), White et al.
patent: 2574537 (1951-11-01), Degroote et al.
patent: 2773068 (1956-12-01), Mannheimer
patent: 2781354 (1957-02-01), Mannheimer
patent: 2820043 (1958-01-01), Rainey et al.
patent: 2846440 (1958-08-01), Hughes
patent: 3152080 (1964-10-01), Stuart et al.
patent: 3187003 (1965-06-01), McBride
patent: 3244724 (1966-04-01), Guttmann
patent: 3555041 (1971-01-01), Katz
patent: 3620807 (1971-11-01), Murray
patent: 3629104 (1971-12-01), Maddox
patent: 3941817 (1976-03-01), Chakrabarti et al.
patent: 4705843 (1987-11-01), Stammann et al.
patent: 4732692 (1988-03-01), Zabotto et al.
patent: 5175220 (1992-12-01), Burba et al.
patent: 5288873 (1994-02-01), Su et al.
patent: 5322630 (1994-06-01), Williams et al.
patent: 5569767 (1996-10-01), Uphues et al.
patent: 5716921 (1998-02-01), Neumiller
Fischer, et al. Tenside Surf. Det. 31, No. 2 (1994) 99-108.
Rosen, M. Geminis: A New Generation of Surfactants Chemtech 30-33 Mar. (1993).
Martell, A., et al. Jacs 73, (12/50) 5357-5361.

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