Process for making pulverulent ammonium polyphosphates stable to

Compositions – Fire retarding – For solid synthetic polymer and reactants thereof

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106 1815, 106 1816, 106 1821, 106 1831, 106 1832, 252610, 521 85, 521106, 521907, 523200, 523208, 523210, 524416, 524594, C09K 2104, C09K 2110, C08K 328, C08K 332

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046393315

ABSTRACT:
The disclosure relates to a process for making a particulate agent stable to hydrolysis based on free-flowing, pulverulent ammonium polyphosphate by treating the ammonium polyphosphate with a thermosetting, artificial resin being water-insoluble when cured. More specifically, the disclosure provides for the ammonium polyphosphate, an aliphatic alcohol as a diluent, and a melamine/formaldehyde-resin or phenol/formaldehyde-resin to be placed in an autoclave and intimately mixed at room temperature; for the mixture to be heated to a temperature of about 80.degree. to about 180.degree. C. and allowed to remain over a period of 15 to 240 minutes at that temperature and under the pressure corresponding to the vapor pressure of the diluent; for the diluent to be separated and for the product so obtained to be dried.

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