Process for making powdered base for formulating curable liquid

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Processes of preparing a desired or intentional composition...

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523213, 523209, 524588, C08K 906

Patent

active

061302724

ABSTRACT:
A process for making a flowable powdered base suitable for use in the formulation of liquid silicone rubber compositions that can be cured to form silicone elastomers. The process comprises (A) fluidizing a reinforcing silica filler in a high-shear mixer, (B) maintaining the content of the mixer at a temperature below about 60.degree. C. while adding to the mixer a silylating agent, a nitrogen containing compound to facilitate the silylation reaction, and water thereby forming an essentially homogeneous mixture comprising a treated reinforcing silica filler; (C) adding a polydiorganosiloxane having a viscosity of about 0.03 to 300 Pa.s at 25.degree. C. to the mixer and forming a flowable powdered base having an average particle size of from about 1 to 1000 microns, and (D) heating the flowable powdered base under conditions sufficient to remove volatiles.

REFERENCES:
patent: 3268473 (1966-08-01), Brown
patent: 3635743 (1972-01-01), Smith
patent: 3824208 (1974-07-01), Link et al.
patent: 4898898 (1990-02-01), Fitzgerald et al.
patent: 5153238 (1992-10-01), Bilgrien et al.

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