Organic compounds -- part of the class 532-570 series – Organic compounds – Phosphorus halides
Patent
1984-12-12
1989-10-03
Killos, Paul J.
Organic compounds -- part of the class 532-570 series
Organic compounds
Phosphorus halides
C07F 942
Patent
active
048714860
ABSTRACT:
Disclosed is a process for producing methylphosphonic dichloride comprising reacting dimethyl methylphosphonate with a chlorinating agent selected from the group consisting of thionyl chloride and phosgene in the presence of a catalytic amount of an inorganic halide selected from the group consisting of ammonium halide and metallic halides where the metal cation is selected from the metals of Groups IA, IIA, IIIB, IVB, VB, VIB, VIIB, VIIIB, IB, IIB and IIIA of the Periodic Table.
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K. Moednitzer and R. E. Miller, "A Convenient One-Step, High Yield Preparation of Methylphosphonyl Dichloride From Dimethyl Memthylphosphonate", Syng. React. Inorg. Metal-Org. Chem. 4(5), pp. 417-427 (1974).
Killos Paul J.
Olin Corporation
Simons William A.
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