Process for making methylcyclopentadienyl manganese tricarbonyl

Details Process for making methylcyclopentadienyl manganese tricarbonyl Process for making methylcyclopentadienyl manganese tricarbonyl

1990-01-12

1990-08-07

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heavy metal containing

C07F 1300

Patent

active

049469754

ABSTRACT:
Cyclopentadienyl manganese tricarbonyl compounds are made by reacting a mixture of 0.25-0.55 moles of manganese acetate and 0.45-0.55 moles of a bis-cyclopentadienyl manganese compound with about 0.5-2.1 moles of an alkyl aluminum compound (e.g. triethyl aluminum) in the presence of about 0.75-1.25 moles of an ether per mole of said alkyl aluminum compound and reacting the mixture with carbon monoxide at about 65.degree.-175.degree. C. and 300-1500 psig.

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patent: 2916505 (1959-12-01), Shapiro
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patent: 2987528 (1961-06-01), Brown et al.
patent: 3260730 (1966-07-01), Hubel et al.
patent: 3288827 (1966-11-01), Kozikowski et al.

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