Process for making fine magnetic ferrite powder and dense ferrit

Plastic and nonmetallic article shaping or treating: processes – Mechanical shaping or molding to form or reform shaped article – Shaping against forming surface

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423594, 252 6256, C01G 4900, C04B 3332

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active

044407130

ABSTRACT:
A manufacturing process for making a finer ferrite powder which can then be used to make a very dense block of the ferrite ceramic. The process for making the powder includes the steps of co-precipitation of an aqueous solution of metal ions and an ammonium oxalate solution. The co-precipitation particles are separated, washed and dried. The particles are low-temperature calcined and then vibro-energy or ball milled and dried. The particles are fluffed and broken up in a blender and pressed into a mold for sintering and pressing in a hot isostatic press procedure. The ferrite blocks are then post annealed in an oxygen atmosphere and cooled to form a dense magnetic ceramic particle. Preferably the process is for use in the production of nickel-zinc ferrite used for magnetic heads.

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Economos, "J. of the Amer. Ceramic Soc.", vol. 38, 1955, pp. 241-244.
Robin, "Bull. Soc. Chim. France", No. 223 (11-12), 1953, pp. 1078-1084.

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