Process for making colloidal sols of antimony pentoxide in polar

Details Process for making colloidal sols of antimony pentoxide in polar Process for making colloidal sols of antimony pentoxide in polar

1975-08-18

1977-04-12

Hayes, Lorenzo B.

Compositions

Inorganic luminescent compositions

Tungsten containing

106 15FP, 252 81, 423617, B01J 1300

Patent

active

040174182

ABSTRACT:
A colloidal dispersion of hydrous antimony pentoxide particles is made by a process which comprises introducing particles of antimony trioxide into a polar organic solvent selected from the group consisting of formamide, methylformamide, dimethyl formamide, acetamide, methylacetamide, dimethylacetamide, dimethyl sulfoxide, formic acid, tetramethyl urea, methanol and ethanol, and contacting said particles with aqueous hydrogen peroxide in the presence of an aliphatic alpha-hydroxy carboxylic acid and a halogen acid selected from the group consisting of hydrogen chloride, hydrogen bromide, and hydrogen iodide at a temperature of from about 0.degree. C to about the decomposition temperature of the reaction mixture for a length of time sufficient to convert at least a portion of the antimony particles to colloidal particles of hydrous antimony pentoxide.

REFERENCES:
patent: 3657179 (1972-04-01), Yates
patent: 3676477 (1972-07-01), Chay et al.
patent: 3860523 (1975-01-01), Petrow et al.

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