Organic compounds -- part of the class 532-570 series – Organic compounds – Azo
Patent
1989-03-29
1990-04-24
Higel, Floyd D.
Organic compounds -- part of the class 532-570 series
Organic compounds
Azo
534575, 534583, 534739, 534839, 534863, 534876, 534887, C09B 2938, C09B 3508, C09B 3700, C09B 4100
Patent
active
049202065
ABSTRACT:
Azo Pigments are made by subjecting a diazo component to an azo coupling reaction with the equivalent quantity of a coupling component difficultly soluble at less than 65.degree. C. in the aqueous/acid and aqueous
eutral pH-ranges. More specifically, an aqueous/acid-solution of the diazo component is continuously mixed at a temperature of less than 65.degree. C. within a period of less than 1 minute with the aqueous/alkaline solution of the coupling component and a predetermined pH between 2 and 9 is established by controlling the flow of the mass streams of diazo component and coupling component; in this way a portion of the coupling component is caused to undergo immediate reaction to the azo pigment to be made whereas the balance portion of the coupling component simultaneously commences precipitating as finely crystalline reactive matter, which is reacted in a post-reaction phase with unreacted diazo component to give the azo pigment to be made.
Behringer Hartmut
Rehberg Heinrich
Higel Floyd D.
Hoechst Aktiengesellschaft
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