Process for making alkylene carbonates

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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549230, C07D31738, C07D31736

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active

043538312

ABSTRACT:
Hexachloroacetone and a vicinal alkylene diol react when heated together in the presence of a weak base to produce chloroform and the cyclic alkylene carbonate. The chloroform distills from the reaction mixture substantially as it is formed and the alkylene carbonate is readily separable from the residual mixture.

REFERENCES:
patent: 4061664 (1977-12-01), Wood
Carl R. Noller, Chemistry of Organic Compounds, 2nd Ed. (1957), pp. 310 and 741.
F. W. Grant et al., Jour. Org. Chem., vol. 25 (1960), pp. 1433-1434.
Kadaba et al., J. Org. Chem., 25, 1431-1433 (1960).
Migaichuk et al., J. Appl. Chem. (USSR transl.), 50, 2471-2473 (1977).

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