Process for leaching particulate solid materials

Chemistry: natural resins or derivatives; peptides or proteins; – Proteins – i.e. – more than 100 amino acid residues – Scleroproteins – e.g. – fibroin – elastin – silk – etc.

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530422, 530423, 530426, 530840, 204233, 75101R, 266101, 502 22, A23J 110, B01D 1102, C07G 700

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active

048249394

ABSTRACT:
A novel leaching process for separating extractable material from a particulate solid material that comprises extractable and non-extractable portions includes the steps of introducing the particulate solid material and a liquid solvent to an extraction zone; agitating the liquid solvent to a degree sufficient to suspend the particulate solid material and effect segregation of particles thereof in relation to their propensity to settle; maintaining contact between the liquid solvent and the particulate solid material for a time sufficient to leach extractable material therefrom; and selectively withdrawing particles of the solid material from the extraction zone. In a preferred embodiment, the leaching process is a multi-stage process in which the selectively withdrawn particles from each stage are introduced to the next successive stage of the series. A particularly important use for the novel leaching process is in the recovery of gelatin from bone, and specifically in that step of the gelatin manufacturing process in which granulated bone is demineralized by contact with a dilute acid solution which converts bone particles to particles of ossein by extracting the minerals from the bone.

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Svanoe, "Krystal Classifying Crystallizer", Ind. Eng. Chem., 32, 636 (1940).
Placho et al., "Counter-Current Solid Liquid Extraction/Cascade of Batch Extractors", The Canadian Jour. Chem. Eng., vol. 50, 611-615, Oct. 1972.
Agarwal et al., "Multistage-Leaching Simulation", Chem. Eng., 135-140, May 24, 1976.
Makarewicz et al., "Kinetics of Acid Diffusion and Demineralization of Bone", The Jour. Photographic Sci., vol. 28, 177 (1980).
H. G. Schwartzberg, "Continuous Countercurrent Extraction in the Food Industry", CEP 76, No. 4, pp. 67-85, 1980.

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