Process for hydrolyzing 5-isothiocyano-5,6-dihydro-dicyclopentad

Details Process for hydrolyzing 5-isothiocyano-5,6-dihydro-dicyclopentad Process for hydrolyzing 5-isothiocyano-5,6-dihydro-dicyclopentad

1980-01-22

1981-04-21

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

C07C 8300

Patent

active

042632269

ABSTRACT:
5-Amino-5,6-dihydro-dicyclopentadiene is prepared by reacting 5-isothiocyano-5,6-dihydro-dicyclopentadiene and an aqueous caustic medium at a temperature in excess of the melting point of 1,3-bis[5-(5,6-dihydro-dicyclopentadiene)]-2-thiourea while establishing and maintaining a pressure sufficient to maintain the water in the reaction mixture in a liquid state.

REFERENCES:
patent: 3088977 (1963-05-01), Segel
patent: 3150183 (1964-09-01), Buntin
patent: 3154579 (1964-10-01), Flanagan
patent: 3238251 (1966-03-01), Williams
patent: 3304167 (1967-02-01), Buntin et al.
"J. Org. Chem.", 34, pp. 616-624, 1969.

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