Powder metallurgy processes – Powder metallurgy processes with heating or sintering – Consolidation of powder prior to sintering
Reexamination Certificate
1999-11-15
2003-03-25
Jenkins, Daniel J. (Department: 1742)
Powder metallurgy processes
Powder metallurgy processes with heating or sintering
Consolidation of powder prior to sintering
C419S040000
Reexamination Certificate
active
06537488
ABSTRACT:
BACKGROUND OF THE INVENTION
1. Field of the Invention
The present invention relates to a process for handling a green compact made by a press machine from a rare earth metal-based magnetic alloy powder such as an Fe—B—R based magnetic alloy powder, wherein R comprises at least one rare earth element. The present invention also relates to a rare earth metal-based magnet produced through such handling process.
2. Description of the Related Art
It is a conventional practice for producing a rare earth metal-based magnet to press a rare earth metal-based magnetic alloy powder into a predetermined shape in a magnetic field by a press machine, and to arrange green compacts produced in the above manner on a sintering support plate to transport them into a sintering furnace, where they are sintered.
In this case, a press machine
10
and a sintering support plate
15
shown in
FIG. 12
are used for the handling of the green compacts made from the rare earth metal-based magnetic alloy powder by the press machine to transport the green compacts to the sintering support plate. The green compacts
1
formed into a predetermined shape from the rare earth metal-based magnetic alloy powder by the press machine are pushed out onto a stage
12
by a push-out means
11
such as pusher and subjected to a powder removing treatment in which a surplus magnetic powder around the green compacts
1
is blown away by a nitrogen gas or the like blown out of a powder removing device
13
. Then, the green compacts are pushed out onto a transporting belt
14
by the push-out means
11
. The green compacts are transported to near the sintering support plate
15
by the transporting belt
14
and then pushed out onto the sintering support plate
15
from the transporting belt
14
by a push-out means
16
such as a pusher. Thus, a large number of the green compacts can be arranged efficiently on the narrow sintering support plate of a simple construction and hence, the above-described steps are repeated, thereby allowing the succeeding green compacts
1
to sequentially push the already transported preceding green compacts to slide them on the sintering support plate
15
, as shown in
FIGS. 13 and 14
. In this manner, all the green compacts
1
are arranged in a final transport position on the sintering support plate
15
. In
FIG. 12
, reference character
10
a
designates an upper punch of the press machine
10
; reference character
10
b
designates a die of the press machine
10
; reference character
10
c
designates a box (feeder) for supplying the magnetic alloy powder to the press machine
10
; and reference character
10
d
designates a magnetic field generating coil.
However, the rare earth metal-based alloy powder such as the Fe—B—R (R comprising at least one rare earth element) based magnetic alloy powder has a large hardness as compared with ferrite. For this reason, if such powder is pressed too strongly, the die is worn. If the powder is pressed at a high pressure, the orientation tends to be disordered, resulting in a degraded magnetic characteristic. Therefore, in order to provide a higher magnetic characteristic pressing force, the pressing pressure can be less risen and hence, the green compacts are liable to brittle and destroyed, as compared with ferrite. Particularly, a rare earth metal-based magnetic alloy powder made by the strip casting process and having an excellent magnetic characteristic has a small average particle size and moreover, has a narrow and sharp particle size distribution. Therefore, green compacts produced from such rare earth metal-based magnetic alloy powder are soft, a poor shaping property, and difficult to handle, as compared with a powder which is made by a mold-casting process and whose particle size distribution varied widely. A green compact made by pressing from a powder containing a lubricant such as an ester of an aliphatic acid added thereto is further brittle.
Because the green compacts are brittle as described above, it is necessary to handle the green compacts carefully by a transporting means such as a transporting belt, a pusher, a robot and the like. Especially, there is a problem that the powder removing treatment is time-consuming, and unless the powder removing treatment for the green compacts made in advance by pressing is finished, the pressing of the subsequent powder cannot be started, resulting in a significantly degraded efficiency of operation of the press machine.
To exhibit the magnetic characteristic sufficiently, it is necessary to conduct the pressing in a high magnetic field of 0.9 to 1.5 T and for this reason, it is necessary to demagnetize the green compacts by a counter magnetic field after the pressing. However, the perfect demagnetization cannot be achieved and for this reason, the powder scattered around the green compact is adsorbed. It is impossible to advance the process without carrying-out of this powder removing treatment and hence, an increase in efficiency of the powder removing treatment is a large subject.
The use of the sintering support plate having a high friction coefficient is preferred in order to ensure that the green compacts are prevented from slipping on the sintering support plate to come into close contact with another green compact, or to become fallen, during transportation of the sintering support plate to the sintering furnace. Particularly, the R—Fe—B based magnet is produced in a liquid-phase sintering manner. For this reason, if a very smooth support plate is used, neodymium (Nd) eluted during the sintering is deposited onto the support plate and hence, it is necessary to use a support plate having a high friction coefficient. For this reason, there is arisen a problem that the green compacts which are slid through a longer distance, i.e., arranged earlier, are cracked at their bottoms, and in a severe case, the green compacts are destroyed before the sintering. To push out the green compacts in a first row, the green compacts, if being pushed by a friction force corresponding to one green compact, can be slid on the support plate. However, it is necessary to push the green compacts in an n-th row by a friction force corresponding to an n-number of green compacts, and such friction force is applied locally to the green compacts in the n-th row. If such friction force is larger than the strength of the green compacts, the green compacts are crushed and destroyed. In addition, the green compacts in the first row are slid through a distance corresponding to the n-rows and for this reason, are chipped at their bottoms.
SUMMARY OF THE INVENTION
Accordingly, it is an object of the present invention to provide a process for handling green compacts made from a rare earth metal-based magnetic alloy powder, wherein the problems associated with the prior art can be eliminated; the deposition of the green compacts to the support plate does not occur, the efficiency of operation of the press machine can be increased, and the cracking and chipping of the green compacts do not occur during movement of the green compacts on the sintering support plate. It is another object of the present invention to provide a rare earth metal-based magnet which is produced through the above handling process.
To achieve the above object, according to a first aspect and feature of the present invention, there is provided a process for handling green compacts made from a rare earth metal-based magnetic alloy powder, comprising the step of sliding, on a sintering support plate, green compacts made from a rare earth metal-based magnetic alloy powder by a press machine, wherein the support plate used has a surface roughness degree Ra in a range of 0.6 to 47 &mgr;m.
According to a second aspect and feature of the present invention, in addition to the first feature, the rare earth metal-based magnetic alloy powder for forming the green compacts contains a lubricant added thereto.
According to a third aspect and feature of the present invention, in addition to the first feature, the rare earth metal-based magnetic alloy powder for formi
Hashikawa Hiroshi
Okumura Shuhei
Armstrong Westerman & Hattori, LLP
Jenkins Daniel J.
Sumitomo Special Metals Co. Ltd.
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