Process for gently cooling and crystallizing melamine from a...

Organic compounds -- part of the class 532-570 series – Organic compounds – Four or more ring nitrogens in the bicyclo ring system

Reexamination Certificate

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C544S201000

Reexamination Certificate

active

07153962

ABSTRACT:
Process for cooling and crystallizing solid melamine from the gaseous phase or from melamine melts as they develop in technical processes used to produce melamine, characterized in that the melamine-containing process gases or melamine melts are introduced into liquid, organic phase at high pressure, said phase comprising polyvalent alcohols such as ethylene glycol, glycerine or their homologous series or of amines such as ethanol amines or a mixture of both groups. The advantage this process is that the hot melamine is cooled very quickly without forming thermal decomposition products and that during quenching no reaction of the melamine with the solvent occurs, the formation of higher deammoniation products such as melam and melem is prevented and higher deammoniation products of the melamine such as melam and melem, are partially converted back into melamine.

REFERENCES:
patent: 2755887 (1956-07-01), Boatright et al.
patent: 5514796 (1996-05-01), Best et al.
patent: 1 035 117 (2000-09-01), None
patent: 1 248 254 (2004-10-01), None
Ullmann's Encyclopedia of Industrial Chemistry, vol. A 16, 5th Edition pp. 171-185 (1990).

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