Process for forming filaments from polyamic acid

Plastic and nonmetallic article shaping or treating: processes – Forming continuous or indefinite length work – Shaping by extrusion

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264236, 4234472, D01F 700

Patent

active

040565980

ABSTRACT:
A process for producing continuous filaments from polyamic acid suitable for conversion to polyimide filaments comprising providing a starting solution consisting essentially of equimolar amounts of P,P-diaminophenyl ether and bis-(3,4-dicarboxyphenyl) sulfone dianhydride, the remainder a solvent selected from the group consisting of dimethylformamide, methyl pyrrolidone and mixtures thereof, said starting solution having a viscosity ranging from 500 to 5,000 centipoises preferably 1,500 to 3,000 centipoises, and forming the starting solution into filaments by extruding it in a coagulating bath consisting essentially of a liquid selected from the group consisting of propanol, methyl alcohol, ethyl alcohol, butyl alcohol, a mixture of ethyl alcohol and propanol and a mixture of methyl alcohol and acetone.

REFERENCES:
patent: 3179614 (1965-04-01), Edwards
patent: 3179630 (1965-04-01), Endry
patent: 3179633 (1965-04-01), Endry
patent: 3528937 (1970-09-01), Reynolds et al.
patent: 3529051 (1970-09-01), Buckley et al.
patent: 3803081 (1974-04-01), Lubowitz
patent: 3812159 (1974-05-01), Lubowitz
patent: 3985934 (1976-10-01), Farrissey et al.

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