Process for fabrication of large titanium diboride ceramic bodie

Plastic and nonmetallic article shaping or treating: processes – Mechanical shaping or molding to form or reform shaped article – Shaping against forming surface

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264 65, 501 98, C04B 3558

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active

048122807

ABSTRACT:
A process for manufacturing large, fully dense, high purity TiB.sub.2 articles by pressing powders with a sintering aid at relatively low temperatures to reduce grain growth. The process requires stringent temperature and pressure applications in the hot-pressing step to ensure maximum removal of sintering aid and to avoid damage to the fabricated article or the die.

REFERENCES:
patent: 3003885 (1961-10-01), Mandorf
patent: 4268314 (1981-05-01), Montgomery
patent: 4543227 (1985-09-01), Biddulph
Ferber, Effect of Microstructure on the Properties of TiB.sub.2 Ceramics, mmunications of the American Ceramic Society, Jan. 1983.
Federer, Fabrication and Characterization of Liquid Metal-Densified Tib.sub.2 Ceramics, ORNL/TM-9572.
Becher, Effect of Residual Nickel Content on the Grain Size Dependent Mechanical Properties of TiB.sub.2, Journal of Materials Science Letters 5, (1986) 195-197.

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