Process for extracting bitter flavoring principles from hops

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07C 4500, C07C 4516, C07C 4524

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active

041607872

ABSTRACT:
A process is described for converting the .alpha.- and .beta.-acids of hops into the iso-.alpha. acids for use as a bitter flavoring principle ingredient for beers. The .alpha.-acids content of the hops is directly isomerized to the iso-.alpha.-acid, the bitter principle ingredient. The .beta. acids in the hops extract is transformed to the .alpha. acid either after a direct separation step before the .alpha.-acid isomerization or the residual .beta.-acids, after the isomerization, are then transformed and the resultant .alpha.-acid is isomerized. The .beta.-acid transformation results from a radiation activation followed by an oxidation step with a per - acid.
The isomerization of the .alpha.-acid to the iso-.alpha.-acid is accomplished by reaction with an alkaline earth metal ethoxide preferably the magnesium ethoxide.

REFERENCES:
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patent: 3354219 (1967-11-01), Rigby
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patent: 3923897 (1975-12-01), Worden
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patent: 4002683 (1977-01-01), Todd
Kuhn, "C,C-Photolytische Aromatisierung von Cyclohexadienonen des Lupulon-Typs", pp. 48-55, 66-79, (1963).

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