Process for electrolytic recovery of titanium metal sponge from

Specialized metallurgical processes – compositions for use therei – Processes – Free metal or alloy reductant contains magnesium

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75121, 423 69, 204 64T, 204 70, C22B 3412, C01G 2302, C25C 328/3/04

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045184267

ABSTRACT:
A process for producing titanium metal sponge within a closed cell system involving the electrical decomposition of molten magnesium chloride into magnesium metal and chlorine gas within a closed cell to form said magnesium metal as a molten layer upon said magnesium chloride; terminating said electrolytic decomposition, and subsequently; directly contacting titanium tetrachloride with said layer of magnesium metal for effecting a reduction reaction therebetween within the same closed cell to form titanium metal sponge and magnesium chloride and removing said titanium metal sponge from said closed cell. The chlorine gas by-product can be used to form titanium tetrachloride from a titanium ore/coke mixture.

REFERENCES:
patent: 2486912 (1949-11-01), Belchetz
patent: 2789943 (1957-04-01), Kittelberger
patent: 2830940 (1958-04-01), Hood
patent: 2858189 (1958-10-01), Globus
patent: 2880156 (1959-03-01), Benner et al.
patent: 2943032 (1960-06-01), Benner
patent: 2951021 (1960-08-01), Pietro
patent: 3021268 (1962-02-01), Egami

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