Chemistry of inorganic compounds – Treating mixture to obtain metal containing compound – Group iiia metal or beryllium
Patent
1977-11-08
1982-01-12
Meros, Edward J.
Chemistry of inorganic compounds
Treating mixture to obtain metal containing compound
Group iiia metal or beryllium
423329, 423332, C01B 3328
Patent
active
043104967
ABSTRACT:
Silicon dioxide containing waste flue dust from the production of silicon metal and silicon alloys is converted to crystalline zeolite molecular sieves of type A by (1) dissolving the flue dust in alkali metal hydroxide solution with the formation of alkali metal silicate solution having a module (SiO.sub.2 :Me.sub.2.sup.I O) in the range of 2.0:1 to 3.5:1 at a temperature of 60.degree.-100.degree. C.; (2) purifying the thus obtained alkali metal silicate solution from organic constituents by treatment with activated carbon and/or an oxidizing agent and separating the non-decomposable residue from the solution; and, (3) reacting alkali metal aluminate solution present at room temperature with the diluted, purified alkali metal silicate solution with a module (SiO.sub.2 :Na.sub.2 O) of 2.0:1 to 3.5:1 obtained by steps (1) and (2) and subsequently crystallizing the reaction mixture ((2.0-4.4)Na.sub.2 O:Al.sub.2 O.sub.3 ; (1.3-1.8)SiO.sub.2 :(90-120)H.sub.2 O) at a temperature of 90.degree.-95.degree. C. for a period of 6-12 hours, subsequently filtering, washing to pH of about 10-11 and drying to recover a crystalline, zeolitic molecular sieve of type A having a degree of whiteness according to Berger (A. Berger, Die Farbe 8 Nr. 4/6 (1959) pages 187-202) at 460.mu. in the range of 90-95%.
REFERENCES:
patent: 2882243 (1959-04-01), Milton
patent: 3017347 (1962-01-01), Kratz
patent: 3489586 (1970-01-01), Chapman
Achenbach Karl
Turk Gunter
Degussa
Meros Edward J.
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