Process for controlling thermal history of Czochralski-grown sil

Single-crystal – oriented-crystal – and epitaxy growth processes; – Processes of growth from liquid or supercritical state – Having pulling during growth

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117 14, 117200, C30B 1520

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active

057797919

ABSTRACT:
A Czochralski method of producing a single crystal silicon ingot having a uniform thermal history from a silicon melt contained in a crucible coaxial with the ingot. In the process the pulling rate of the end-cone of the ingot is maintained at a relatively constant rate which is comparable to the pulling rate for the second half of the main body of the ingot. During the pulling of the end-cone of the crystal at a constant rate, the process may be further refined by, either independently or in combination, increasing the heat supplied to the melt, reducing the crystal rotation rate and/or reducing the crucible rotation rate. The second half of the main body of a single crystal silicon ingot grown in accordance with this process exhibits a relatively uniform axial concentration of flow pattern defects and amount of oxygen precipitated.

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M. Hourai, T. Nagashima, E. Kajita, S. Miki, S. Smita, M. Sano and T. Shigematsu, "Oxygen Precipitation Behavior In Silicon During Czochralski Crystal Growth," in Semiconductor Silicon 1994, pp. 156-167, Eds., H.R. Huff, W. Bergholz and K. Sumino (Princeton, NJ; The Electrochem. Soc., 1994).
H. Harada, T. Abe and J. Chikawa, "Oxygen Precipitation Enhanced With Vacancies In Silicon," Semiconductor Silicon 1986, pp. 76-85, Eds., H.R. Huff, T. Abe and B.O. Kolbesen Pennington, NJ; The Electrochem Soc., 1986) .

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