Process for continuous production of full esters of polyols

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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560233, C07C 6738

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active

042448824

ABSTRACT:
Full esters of polyols selected from pentaerythritol and polypentaerythritols are continuously produced by (i) continuously introducing a solution of the polyols in pyridine bases, olefins having at least 4 carbon atoms in an amount of at least 0.4 equivalent per 1.0 equivalent of the hydroxyl group in the polyols, a catalyst containing cobalt carbonyls and pyridine bases, and carbon monoxide, into a reaction zone from one end thereof in such an amount of the pyridine bases as is within the range of from 40 to 70% by weight based on the total amount of the pyridine bases, the polyols and the olefins; (ii) introducing an additional amount of the olefins into at least one middle portion of the reaction zone, and; (iii) continuously withdrawing the resultant reaction mixture from the other end of the reaction zone.

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patent: 3883587 (1975-05-01), Isa
patent: 3891683 (1975-06-01), Isa
patent: 3935228 (1976-01-01), Keblys
patent: 3946055 (1976-03-01), Isa
patent: 3974194 (1976-08-01), Isa
patent: 3980683 (1976-09-01), Isa
patent: 4041057 (1977-08-01), Fanning

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