Process for continuous polycondensation of terephthalic acid and

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From carboxylic acid or derivative thereof

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528272, C08G 6302, C08G 6378, C08G 6382

Patent

active

051985306

ABSTRACT:
Process for continuous production of polyesters by esterification of terephthalic acid with 1,4-bis(hydroxymethyl)cyclohexane with a split feed in the presence of a titanium catalyst at 265.degree. to 305.degree. C. and 0.8 to 1.5 bar up to a conversion of 98.0% to 99.0%, then performing precondensation at 290.degree. to 305.degree. C. and 0.01 to 1.5 bar up to a conversion of 99.4% to 99.7% and finally performing polycondensation at 295.degree. to 310.degree. C. and less than 1.5 mbar up to a conversion corresponding to 50% to 95% of the maximum possible viscosity after adding more titanium catalyst.

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