Process for coagulation and washing of polybenzazole fibers

Plastic and nonmetallic article shaping or treating: processes – Forming continuous or indefinite length work – Shaping by extrusion

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26433111, 264341, 264343, 264344, 264345, 528293, D01F 600

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active

053934784

ABSTRACT:
Fibers spun from polybenzazole dopes can quickly be washed to remove polyphosphoric acid by a combination of initially washing with an acidic liquid and second washing with a hot leaching fluid at at least about 60. The process can reach acceptable residual phosphorous levels (1500-2000 ppm) in as little as about 2 or 3 minutes.

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W. W. Adams et al., AFWAL-TR-864011, Processing, Properties, Structure, and Morphology of PBO and ABPBO Polymer Fibers, Aug. 1986.

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