Process for alkylating and smiles rearrangement of hydroxy aroma

Details Process for alkylating and smiles rearrangement of hydroxy aroma Process for alkylating and smiles rearrangement of hydroxy aroma

1997-03-18

1998-10-06

Kumar, Shailendra

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

564218, 552286, 549 57, C07C23306, C07C23108

Patent

active

058178740

ABSTRACT:
The present invention is a process of converting a hydroxy aromatic into a 2-hydroxy-N-arylacetamide, comprising:
(1) treating a reaction mixture comprising a salt of a hydroxy aromatic with an alkylating agent; and
(2) treating the reaction mixture with a Smiles solvent system and raising the temperature of the reaction mixture.

REFERENCES:
S. Ramsby et al., J. Med. Chem., 32:1198-1201 (1989).
Coutts, et al., J. Chem. Soc. Perkin Trans. 1 (1990) pp. 767-771.
R. Bayles, et al., Synthesis, 31:31-33, (1977).
R. Bayles, et al., Synthesis, 31:33-34, (1977).

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