Process for acylation or alkylation of aromatic compounds in hyd

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

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568323, C07C 4545

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active

051854694

ABSTRACT:
A continuous process is disclosed for the acylation or alkylation of aromatic compounds in hydrogen fluoride. The aromatic compound is sufficiently insoluble in hydrogen fluoride that a two phase reaction medium forms. However, surprisingly, the product acylated or alkylated aromatic compound is soluble in hydrogen fluoride. The present invention particularly relates to use of a continuous, multi-stage process for carrying out the acylation or alkylation reaction. In the multi-stage process, the continuous phase can be either the hydrogen-fluoride rich phase or the aromatic compound-rich phase. The movement of the continuous phase relative to the non-continuous (dispersed) phase can be countercurrent or concurrent. The multi-stage process can be operated in a manner such that the aromatic compound feed to the reaction is entirely consumed or such that unreacted aromatic compound is recycled.

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Doklady Akademii Nauk USSR, 95(2), 297-299 (1954).
Baddely et al., Journal of the Chemical Society, 4943-4945 (1956).
Zhurnal Fizicheskoi Khimii, 31, 1377-1386 (1957).

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