Process and reagent for determining the activity of chymotrypsin

Chemistry: molecular biology and microbiology – Measuring or testing process involving enzymes or... – Involving hydrolase

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435 24, 435 4, 435803, 435188, 436174, 436177, C12Q 137, C12Q 100, G01N 3000

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active

052504182

ABSTRACT:
The present invention provides a process for the determination of the activity of chymotrypsin or trypsin in feces by measurement of the rate of fission of an appropriate substrate by a fecal suspension in an aqueous or aqueous-organic medium, wherein a fecal sample is suspended in the presence of a surface-active agent.
The present invention also provides a reagent for carrying out this process, comprising a surface-active agent, an enzyme substrate and an aqueous salt solution, said reagent having a pH value of from 7 to 11.

REFERENCES:
patent: 4282001 (1981-08-01), Klose et al.
Haverback, B., et al. "Measurement of Trypsin and Chymotrypsin in Stool", Gastroenterology, 44, pp. 588-597 (1963).
Del Mar, E. G., et al., "A Sensitive New Substrate for Chymotrypsin," Analytical Biochemistry, 99, pp. 316-320 (1979).
Kaspar, P., et al., "A New Photometric Method for the Determination of Chymotrypsin in stool," Fresenius Z Anal Chem, 311 (1982) 391-92.
Goldberg, D. M., et al., "Binding of trypsin and chymotrypsin by human intestinal mucosa," Biochim. Biophys. Acta., 167, pp. 613-615 (1968).
Remtulla et al., "Is Chymotrypsin Output a Better Diagnostic Index than the Measurement of Chymotrypsin in Random Stool?", Enzyme 39, 190-8 (1988).
Goldberg et al.; "Fate of Trypsin and Chymotrypsin in the Human Small Intestine", Gut 10, 477-83 (1969).
Kaspar et al., "New Photometric Assay for Chymotrypsin in Stool," Clin. Chem. 30, 1753-7 (1984).
Kaspar et al., "The Distribution of Chymotripsin within the Feces and Description of a New Device for the Preparation of Stool Samples", Clin. Chem. 30, 1864-6 (1984).
Remtulla et al., "Stool Chymotrypsin Activity Measured by a Spectrophotometric Procedure to Identify Pancreatic Disease in Infants", Clin. Biochem. 19, 341-7 (1986).
Durie et al., "Biochemical Tests of Pancreatic Function in Infancy and Childhood", Adv. Clin. Enzymol. 4, 77-92 (1986).

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