Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof
Patent
1985-11-06
1987-03-24
Killos, Paul J.
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acids and salts thereof
C07C 5142
Patent
active
046526757
ABSTRACT:
Process for purifying benzoic acid obtained by oxidation of toluene with a gas containing molecular oxygen, which purification is carried out at a pressure of at least 3 MPa by means of a supercritical extraction using a gas or gas mixture the critical temperature of which is lower than 435 K. The process being characterized in that the benzoic acid to be purified is supplied in a liquid state to a crystallizer in which the prevailing temperatures is below the solidification temperature of the benzoic acid and in which the benzoic acid is treated during and possibly after the crystallization process with the said gas or gas mixture.
REFERENCES:
patent: 2255421 (1941-09-01), Groll et al.
patent: 4227018 (1980-10-01), Wolf et al.
patent: 4539425 (1985-09-01), Kleintjens et al.
patent: 4547587 (1985-10-01), Kleintjens et al.
Goorden Josephus J. P. M.
Kleintjens Ludovicus A. L.
Simons Antonius J. F.
Killos Paul J.
Stamicarbon B.V.
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