Process and apparatus for carrying out the first stage of separa

Distillation: processes – separatory – Plural distillations performed on same material – Distillation of initial distillate

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203 99, 564499, B01D 314

Patent

active

043870058

ABSTRACT:
The present invention relates to a process for carrying out the first stage of separation of constituents of a reaction mixture obtained during synthesis of asymmetric dimethylhydrazine by the Raschig method, consisting in sending, into an empty central section (B) of a column, the reaction mixture coming from said synthesis, this central section being surmounted by a column (C) in which is effected separation of the volatile compounds contained in said mixture and being extended downwardly by an exhausting section (A).

REFERENCES:
patent: 3098017 (1963-07-01), Walter et al.

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