Procedure for the preparation of nitroxyl radicals of sterically

Details Procedure for the preparation of nitroxyl radicals of sterically Procedure for the preparation of nitroxyl radicals of sterically

1991-11-29

1993-06-08

Lee, Mary C.

Organic compounds -- part of the class 532-570 series

Organic compounds

Chalcogen in the nitrogen containing substituent

546113, 546184, 546186, 546242, 548490, 548537, 548570, 548542, 548579, C07D26530, C07D21102, C07D20904, C07D20706

Patent

active

052181162

ABSTRACT:
Procedure for the preparation of nitroxyl radicals of sterically hindered amines, consisting of the reaction of amines with hydrogen peroxide in the presence of a titanium containing catalyst, particularly in the presence of titanium silicalites.
The catalyst can be recovered at the end of the reaction and recycled.

REFERENCES:
patent: 2695301 (1954-11-01), Blicke
patent: 4201721 (1980-05-01), Hallgren
patent: 4792623 (1988-12-01), Sun

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