Procedure for preparing...

Organic compounds -- part of the class 532-570 series – Organic compounds – Unsubstituted hydrocarbyl chain between the ring and the -c-...

Reexamination Certificate

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Reexamination Certificate

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07807827

ABSTRACT:
The invention relates to a procedure for preparing quetiapine by reaction between a compound of formula (II) and a compound of formula (III), in which X means a leaving group and P a protective group of alcohols resistant to alkaline conditions, in the presence of a base, followed by a step of deprotection and, optionally, obtaining a pharmaceutically acceptable salt thereof.Said procedure permits the obtaining of quetiapine with a high degree of purity under soft temperature conditions, with short reaction times and avoiding the use of toxic solvents.(Graphic)

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Warawa E J et al.: “Behavioral approach to nondyskinetic dopamine antagonists: Identification of Seroquel” Journal of Medicinal Chemistry, American Chemical Society. Washington, US, vol. 44, Feb. 1, 2001, pp. 372-389, XP002213291 ISSN: 0022-2623.
Lambert, T.N. et al.: “Synthesis of 3-Hydroxy-2-pyridinone Derivatives of 4-tert-Butylcalix'4lareness: A New Class of Selective Extractants of Actinide(IV) Ions” Journal of Organic Chemistry, vol. 64, 1999, pp. 6097-6101, XP002317244.
Greene. Protective Groups in Organic Synthesis, 3rdedition, Wiley Intemscience, chapter 2, pp. 17-23; 48-51; 54-55; 76-87; 102-105; 110-111; 702-703; 706-708, 2002.
Smith et al. March's Advanced Organic Chemistry, 5thedition, New York (USA): John Wiley & Sons; 2001, p. 446.

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