Pretreatment method for the synthesis of carbon nanotubes...

Chemistry of inorganic compounds – Carbon or compound thereof – Elemental carbon

Reexamination Certificate

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C423S447200, C977S700000, C977S742000, C502S182000

Reexamination Certificate

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08029759

ABSTRACT:
Carbon nanostructures such as multiwalled carbon nanotubes are formed from electrolyzed coal char. The electrolyzed coal char is formed by forming a slurry of coal particles, metal catalyst and water and subjecting this to electrolysis, which generates carbon dioxide and hydrogen. This forms a coating on the particles which includes metal catalysts. These particles can be used as is for formation of multi-walled carbon nanotubes using a pyrolysis method or other method without the addition of any catalyst. The gelatinous coating can be separated from the char and used as a fuel or as a carbon source to form carbon nanostructures.

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International Search Report and Written Opinion, mailed May 11, 2010.
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Premium carbon products and organic chemicals from coal, Profiles, Oct. 2005, PF 05-05.

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