Preservation of dicarboxylic acid chlorides

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07C 5142, C07C 5158

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041827287

ABSTRACT:
Discoloration of dicarboxylic acid chlorides having 4 to 10 carbon atoms, especially those made by reacting the corresponding dicarboxylic acid with phosphorus trichloride, is inhibited by the addition of a dicarboxylic acid thereto. Addition of a dicarboxylic acid to a dicarboxylic acid chloride which has already discolored precipitates impurities and thus clarifies the dicarboxylic acid chloride. The clarified dicarboxylic acid chlorides are useful as starting materials to make polyester foam materials.

REFERENCES:
patent: 1936739 (1933-11-01), Townend

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