Preparation of titanosilicate zeolite TS-1

Chemistry of inorganic compounds – Zeolite – Organic compound used to form zeolite

Reexamination Certificate

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C423S700000, C423S702000, C423S705000, C423S706000, C423S707000, C423S708000, C502S060000

Reexamination Certificate

active

07837977

ABSTRACT:
A method is disclosed for preparing crystalline titanosilicate zeolite TS-1 from a reaction mixture containing only sufficient water to produce zeolite TS-1. In one embodiment, the reaction mixture is self-supporting and may be shaped if desired. In the method, the reaction mixture is heated at crystallization conditions and in the absence of an added external liquid phase, so that excess liquid need not be removed from the crystallized product.

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