Preparation of thioethers

Details Preparation of thioethers Preparation of thioethers

1978-09-25

1981-05-12

Hollrah, Glennon H.

Organic compounds -- part of the class 532-570 series

Organic compounds

Sulfur containing

568 58, C07C14930

Patent

active

042673755

ABSTRACT:
Thioethers may be prepared by reacting a thiol, such as thiophenol, with an alcohol (having electron donor groups in the alpha or beta position to its hydroxyl group) such as phenyl-1-hydroxy-phenethylsulfide. Reaction is carried out in the presence of a Lewis Acid metal halide, typically zinc chloride.

REFERENCES:
patent: 2745878 (1956-03-01), Mavity
I. Ruderman et al., J. Amer. Chem. Soc., 71, pp. 2264-2265, (1949).
Morrisson and Boyd, Organic Chemistry, 2nd edition, (1967), pp. 29-30.
T. Todsen et al., J. Amer. Chem. Soc., 72, pp. 4000-4002, (1950).
Berichte Deutsch. Chemie, vol. 1, pp. 587-591, (1935), Berlin.
D. Gregg et al., J. Org. Chem., pp. 246-252, (1950).
M. Malinovskii, Epoxides and Their Derivatives, pp. 131-136, (1965), Jerusalem, Daniel Davey & Co.

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