Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Mixing of two or more solid polymers; mixing of solid...
Reexamination Certificate
2005-06-27
2010-02-02
Zemel, Irina S (Department: 1796)
Synthetic resins or natural rubbers -- part of the class 520 ser
Synthetic resins
Mixing of two or more solid polymers; mixing of solid...
C525S192000, C525S203000, C525S216000, C525S232000, C525S240000, C525S241000, C525S242000, C525S263000, C264S425000
Reexamination Certificate
active
07655728
ABSTRACT:
The invention relates to a method of preparing a thermoplastic vulcanizate comprising: a) melt processing a blend of thermoplastic polymer and vulcanizable elastomer in a multi-screw extruder having at least three intermeshing screws, wherein said screws have 3-170 mixing zones, and said extruder having a L/D ratio of 15-100, and a screw profile that has 3 to 17 meshes per L/D; b) adding at least one curing agent to the melt-processed blend of a) in at least one location in the first 46% of the length of said extruder, or adding at least one curing agent to the melt-processed blend of a) in a second extruder, so as to initiate curing of the blend: and, curing at least partially said elastomer by reactive melt processing. Improved processing, reaction kinetics and efficiencies are achieved, as well as thermoplastic vulcanizate products having decreased weight gain when placed in mineral oils.
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Cheng Jianya
DeYoung Ronald
Nadella Hari P.
Shen Kuo-Shein
ExxonMobil Chemical Patents Inc.
Zemel Irina S
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