Preparation of tetramethyldisilane from 1,2-tetramethyldichlorod

Details Preparation of tetramethyldisilane from 1,2-tetramethyldichlorod Preparation of tetramethyldisilane from 1,2-tetramethyldichlorod

1980-07-28

1981-09-22

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Silicon containing

C07F 708

Patent

active

042911672

ABSTRACT:
A process of producing tetramethyldisilane by reacting tetramethyldichlorodisilane with a reducing mixture of NaH and NaBH.sub.4 in the presence of a complexing ether such as the diethyl ether of tetraethylene glycol.

REFERENCES:
patent: 3029128 (1962-04-01), Chamberlain
patent: 3312605 (1967-04-01), Braithwaite
patent: 3639105 (1972-02-01), Atwell et al.
patent: 3983224 (1976-09-01), Allain et al.
patent: 4052430 (1977-10-01), Yajima et al.
patent: 4146657 (1979-03-01), Gordon
Schlesinger, "J.A.C.C.", 75, p. 186, 1953.
"J. Organomotac. Chem.", 6, pp. 202-204, 1966.

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