Preparation of sub-micron metal oxide powders from chloride-cont

Details Preparation of sub-micron metal oxide powders from chloride-cont Preparation of sub-micron metal oxide powders from chloride-cont

1976-06-30

1977-11-15

Meros, Edward J.

Chemistry of inorganic compounds

Oxygen or compound thereof

Metal containing

423598, 252 6259, 252 6263, 252 635, 106 733, 106 7331, 252 629, C01G 4900, C01G 2300

Patent

active

040585921

ABSTRACT:
Sub-micron metal oxide powders, such as barium titanate, are prepared by mixing a carbohydrate material with solution of barium and titanium compounds, and in some instances other metal compounds, followed by ignition and calcining of the mixture to give sub-micron size particles of barium titanate loosely held together in friable aggregates. For economic reasons as well as their commercial availability, inorganic chlorides are suitable for use as one or more of the starting compounds. However, the presence of a chloride compound greatly influences the thermal stability of that compound in the mixture and hence its rate of decomposition was found to be slow. Accordingly, after the ignition step any chlorides present in the mixture are removed before calcination. The process provides a means for the direct formation of barium titanate free of unwanted phases and which is chemically pure. Barium titanate can also be prepared as an intimate mixture or as a solid solution with other oxides.

REFERENCES:
patent: 2758911 (1956-08-01), Lynd
patent: 3049404 (1962-08-01), Wade
patent: 3549315 (1970-12-01), Lester
patent: 3634254 (1972-01-01), Micheli
patent: 3826755 (1974-07-01), Grimes
patent: 3862046 (1975-01-01), Walker

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