Preparation of specifically adjusted polyalcohol mixtures based

Compositions – Compositions containing a single chemical reactant or plural... – Organic reactant

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25218225, 25218227, C09G 300

Patent

active

048615137

ABSTRACT:
A polyalcohol mixture is produced by heating dehydrating a reaction mixture comprising D-sorbitol, L-sorbitol or a mixture thereof in the presence of an acid catalyst. The reaction progress is followed by measuring the optical rotation of the reaction mixture during the reaction. The reaction is stopped when the optical rotation value of the reaction mixture corresponds to the optical rotation value of the desired polyalcohol mixture.

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Shoemaker et al, "Experiments in Physical Chemistry", pp. 419-421, McGraw-Hill Book Co. Inc. (1962) New York.
Perry et al, "Chemical Engineers' Handbook", 5th Ed., p. 22-2, 47, 49, McGraw-Hill Book Co. (1973) New York.

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