Preparation of reactive metal hydrides

Chemistry of inorganic compounds – Hydrogen or compound thereof – Binary compound

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423DIG12, 204164, C01B 602

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active

047285079

ABSTRACT:
Transition metal, notably zirconium alloy, is melted (e.g., by a plasma) to form droplets within the size range of minus 20, plus 60 mesh. The droplets are exposed to a hydrogen atmosphere for a short period while cooling through the hydriding temperature range (e.g., 600.degree. C. to 400.degree. C.). A friable particulate of uniform size and hydrogen content, suitable for sintering or forming components, is recovered.

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Airco, Manual of Carbon and Graphite, Air Reduction Company, 1968, pp. 128-129.

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