Preparation of quaternary ammonium thiomolybdates

Details Preparation of quaternary ammonium thiomolybdates Preparation of quaternary ammonium thiomolybdates

1980-12-05

1982-08-10

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07F 1100

Patent

active

043437478

ABSTRACT:
Quaternary ammonium thiomolybdates are prepared in a two-phase reaction system by contacting an aqueous solution of a thiomolybdate salt with a solution of a quaternary ammonium salt in a water-immiscible organic solvent. For example, mixing a solution of dicocodimethylammonium chloride in toluene with an aqueous solution of potassium thiomolybdate results in a toluene solution containing dicocodimethylammonium thiomolybdate.

REFERENCES:
patent: 2909541 (1959-10-01), Hugel
patent: 3489775 (1970-01-01), de Roch et al.
Krause et al. JACS 47, 1689-1694, (1925).

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