Preparation of polysulfide compositions

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From sulfur-containing reactant

Reexamination Certificate

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Details

C528S387000, C528S373000, C528S377000, C528S482000, C528S486000, C568S021000

Reexamination Certificate

active

06939941

ABSTRACT:
A process is provided for the manufacture of liquid polysulfide polymers. In particular, the process allows for making the liquid form of the polysulfide polymer directly and eliminates the need to first make a solid polysulfide polymer and then convert it to a liquid.

REFERENCES:
patent: 5430192 (1995-07-01), Hobbs et al.
patent: 56090835 (1979-12-01), None
patent: 04046931 (1990-06-01), None
George R. Pettit, “Preparation of Elastothiomers with a Phase Transfer Catalyst,” Journal of Polymer Science: Polymer Chemistry Edition, vol. 18, p. 345-347, 1980.
Tatsuro Matsui et. al., “Detection of a New Crosslinking and Properties of Liquid Polysulfide Polymer,” Journal of Applied Polymer Science, vol. 71, p. 59-66, 1999.
Yoshio Imai et. al., “Synthesis of Aliphatic Polysulfides by Phase-Transfer-Catalyzed Polycondensation of Dibromoalkanes with Dithiols,” Journal of Polymer Science: Polymer Letters Edition, v. 17, p. 579-583, 1979.
Mitsuru Ueda, et. al., “Synthesis of Poly(aliphatic sulfides) by Polycondensation of Sodium Sulfide with Dibromoalkanes in the Presence of quarternary Onium Salts,” Macromolecules, v. 15, p. 248-251, 1982.
W. Mazurek et.al., “13C NMR of Polysulfide Prepolymers,”Macromolecules, vol. 24, p. 3261-3265, 1991.

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