Preparation of pigmentary 2,9-dichloroquinacridone

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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546 56, C09B 4800

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active

054244293

ABSTRACT:
A process for the direct preparation of pigmentary 2,9-dichloroquinacridone, which comprises oxidizing 2,9-dichloro-6,13-dihydroquinacridone directly to pigmentary 2,9-dichloroquinacridone by heating a reaction mixture comprising 2,9-dichloro-6,13-dihydroquinacridone, an alkali metal hydroxide, a water-soluble organic solvent, water and effective amounts of an oxidizing agent and a phthalimidomethylquinacridone particle growth inhibitor. The process yields pigmentary 2,9-dichloroquinacridone directly; without the need for additional particle-size reducing aftertreatments.

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